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Cannabidiol is one of the main non-psych...
The invention relates to a cannabidiol d...
The influence of different 5-alkyl-subst...
The present invention relates to certain...
di-methyl ether of 5-n-butyl-resorcinol
5-n-butyl-1,3-dihydroxybenzene
| Conditions | Yield |
|---|---|
|
With
boron tribromide;
In
dichloromethane;
at 0 - 20 ℃;
|
78% |
|
di-methyl ether of 5-n-butyl-resorcinol;
With
boron tribromide;
In
dichloromethane;
at -15 - 20 ℃;
for 2h;
Inert atmosphere;
With
water;
In
dichloromethane;
|
75% |
|
With
boron tribromide;
In
dichloromethane;
at 0 - 20 ℃;
for 20h;
Inert atmosphere;
|
65% |
|
With
hydrogen iodide;
|
|
|
With
chloro-trimethyl-silane; sodium iodide;
In
acetonitrile;
for 36h;
Heating;
|
2,4-dihydroxy-6-n-butylbenzoic acid
5-n-butyl-1,3-dihydroxybenzene
| Conditions | Yield |
|---|---|
|
In
methanol; water;
at 60 ℃;
for 5h;
|
80% |
di-methyl ether of 5-n-butyl-resorcinol
2,4-dihydroxy-6-n-butylbenzoic acid, methyl ester
3,5-dimethoxybenzaldehdye
3,5-dimethoxybenzoic acid
(6aR,10aR)-3-butyl-6,6,9-trimethyl-6a,7,10,10a-tetrahydro-6H-benzo[c]chromen-1-ol
CBD
